The results of laboratory and industrial scale trials of saltpeter type nitrogen-sulfur fertilizers from different origin calcium sulfate hydrates as sulfur sources was presented.The tech. powd. gypsum and gypsum and anhydrite minerals were used.During trials, the optimal milling, drying and granulating parameters were determinedFrom industrial scale trials, the products containing 27.3% N and 2.5-5.5% S with very good mech. properties were obtained.